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Practical Instrumental Analysis


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Table of Contents

IINTRODUCTION Analytical Chemistry - The History Analytical Chemistry and Its Role in Today's Society INTRODUCTION TO QUALITY MANAGEMENT Historical Background Variability The Four Pillars of Wisdom (from Shewhart to Deming) Zero-Defect Tolerance Why Standards? The Controlled Process ISO Guidelines 9004 Quality Management System (QMS) Requirements FUNDAMENTALS OF STATISTICS Basic Concepts Important Terms Quality of Results (Accuracy and Precision) Regression THE ANALYTICAL PROCESS The Analytical Process in the Overall Context Planning Phase Analysis Assessment Validation Final Documentation EXAMPLE OF A VALIDATION STRATEGY Determination of Phenol in Industrial Waste Water ORGANIZATIONAL AND PRACTICAL PROCEDURES IN THE TEACHING LABORATORY PROGRAM Goals Safety in the Laboratory Class Experimental Project Workflow Reports LITERATURE Cited Literature Recommended Norms (Selection) Suggested Books (Selection) PROJECTS Chromatography Spectroscopy Electrophoretic Separation Methods Automation Mass Analytical Determination Methods General Analytical Methods 7 Universal Separation Methods APPENDIX A SELECTION OF RECOMMENDED SOURCES BY SUBJECT AREA APPENDIX B STATISTICAL TABLES APPENDIX C OBLIGATORY DECLARATION FOR STUDENTS APPENDIX D THE INTERNATIONAL SYSTEM OF UNITS (SI) - AND THE 'NEW SI' APPENDIX E EVALUATION GUIDE FOR FORMAL REPORTS APPENDIX F SAFETY IN THE ANALYTICAL LABORATORY INDEX

About the Author

After his apprenticeship, Sergio Petrozzi worked as a chemical lab technician at the Laboratory of Physical Chemistry ETHZ (Swiss Federal Institute of Technology) and at the Swiss Federal Institute of Aquatic Sciences and Technology (EAWAG), Switzerland. After acquiring his federal diploma (Diplom Hohere Fachprufung), he joined the Institute of Chemical Engineering ETHZ where he gained great experience as teaching assistant in laboratory courses. His daily routine focused among other topics, on the following topics at the ETHZ in Zurich: Development, optimization and validation of analytical methods. He subsequently worked as an application chemist at Buchi Labortechnik AG, Flawil (Switzerland) with a focus on the validation of applications for environmental determinations. He has authored numerous publications in international journals and is presently employed as a Scientific Associate at the Zurich University of Applied Sciences ZHAW, Wadenswil (Switzerland), where, among other things, he is teaching adviser in analytical chemistry laboratory at the Institute for Chemistry and Biological Chemistry (ICBC).

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